BL-4A Trace element analysis/X-ray microbeam station
Contact person:Yasuhiro Niwa
  5444(PHS:4942)
  yasuhiro.niwa@kek.jp
Yoshio Takahashi (Univ. Tokyo)  
1.Outline
This station is mainly used for X-ray fluorescence analysis  with X-ray (semi-) microbeam including ultra trace element analysis, chemical  state analysis, and elemental and chemical state mapping. Since synchrotron X-ray fluorescence analysis  is highly sensitive to trace elements and has non-destructive nature, it is  suitable for the analysis of the biological, biomedical, environmental and  geological samples. It is beneficial for materials science as well. 
  
  A constant exit double crystal monochromator is  equipped for the experiments with monochromatic X-rays.  The experimental hutch is located 13  m from the source point.

  
  Schematic view of the beamline 
  2. Area of Research
  
  X-ray fluorescence analysis with X-ray (semi-)microbeam
  trace          element analysis / chemical          state analysis (XANES) / elemental (chemical state) mapping / 
  3. Light Source & X-rays at sample
  
| Light source: Bending magnet | (σ:0.247mm(H) ×0.088 mm (V)) | 
| Energy range | Monochromatic X-rays. 6-18 keV | 
| Energy resolution(ΔE/E) | 10-4(monochromatic X-rays) | 
| Beam size | Microbeam, 5μm × 5μm with KB  optics | 
| Photon flux | monochromatic beam(max) 1010 photons/s | 
 
  
  4. Facilities in Experimental Station
  
  5. Main features of X-ray fluorescence analysis
  
  
1) Micorbeam analysis
2) Poly-Capillary analysis

X-ray microbeam system
  
  6. References
  
  1) A.Iida and T.Noma: Nucl. Instrum. and Methods,  B82(1993)129.
Last modified: 2014-08-25