BL-4A Trace element analysis/X-ray microbeam station

Contact person:Yasuhiro Niwa
5444(PHS:4942)
yasuhiro.niwa@kek.jp
Yoshio Takahashi (Univ. Tokyo)


1.Outline

This station is mainly used for X-ray fluorescence analysis with X-ray (semi-) microbeam including ultra trace element analysis, chemical state analysis, and elemental and chemical state mapping. Since synchrotron X-ray fluorescence analysis is highly sensitive to trace elements and has non-destructive nature, it is suitable for the analysis of the biological, biomedical, environmental and geological samples. It is beneficial for materials science as well.

A constant exit double crystal monochromator is equipped for the experiments with monochromatic X-rays. The experimental hutch is located 13 m from the source point.

 

 



Schematic view of the beamline


2. Area of Research


X-ray fluorescence analysis with X-ray (semi-)microbeam
trace element analysis / chemical state analysis (XANES) / elemental (chemical state) mapping /


3. Light Source & X-rays at sample

Light source: Bending magnet (σ:0.247mm(H) ×0.088 mm (V))
Energy range Monochromatic X-rays. 6-18 keV
Energy resolution(ΔE/E) 10-4(monochromatic X-rays)
Beam size

Microbeam, 5μm × 5μm with KB optics
Semi-microbeam 30μmφwith a poly-capillary

Photon flux monochromatic beam(max) 1010 photons/s



4. Facilities in Experimental Station



5. Main features of X-ray fluorescence analysis


1) Micorbeam analysis

2) Poly-Capillary analysis

X-ray microbeam system



6. References


1) A.Iida and T.Noma: Nucl. Instrum. and Methods, B82(1993)129.


Last modified: 2014-08-25